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Heidolph rotary evaporators, 100-760 torr, 20-100°C. BÜCHI R-124 rotary evaporator for synthesis, 0.10-760 torr, 20-260°C. Mettler Microbalances, 0.01 mg resolution. Labconco high-vacuum drying and lyophilization. Analytical Equipment. TA Instruments DSC250, Differential Scanning Calorimeter, -90°C-550°C. TA Instruments Discovery Series TGA-MS; 0.1-500°C/minimum in linear control or up ...
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School Georgia State University; Course Title CHEM 2400; Uploaded By cdinh92. Pages 15. This preview shows page 13 - 15 out of 15 pages. 21) Concentrate the caffeine extract by rotary evaporation. Leave the flask open in your drawer until next week to air dry the crude product. Next Week-Sublimation Process 1) Work in groups of four. 2) Combine the weighed crude caffeine from the 4 students ...
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Evaporation of bound solvent. Some solvents tend to stick to the solid particles by physical bridging, or to hide in the pores of the particle structure, while others don’t. In order to predict required process times, detailed knowledge of the separation behavior is critical. Cooling. For safe discharge, it might be required to cool the solids to very low temperatures prior to discharge ...
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Rotary evaporators are mainly used to evaporate light boiling components under normal pressure or vacuum. When used in pilot plant and small scale production they are also suitable for semi-continuous evaporation. They are characterized by providing a gentle thermal treatment for temperature-sensitive mediums and provide a higher evaporation rate as non-stirred glass distillation flasks ...
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Rotary evaporation, equipped with a bump trap, under vacuum at ambient temperature. Application is restricted to macroanalysis. 3. Evaporation on a hot plate in an Erlenmeyer flask with or without a modified Snyder column, in which the solution is heated at 30°C. Macro and microanalysis. 4. Heated nitrogen blowdown in an Erlenmeyer flask, in which the solution is heated at 30°C with a gentle ...
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• Rotary evaporator with vertical glass condenser for distillation of solvents with higher boiling points. 20% narrower than RE300 saving space. • Rotary evaporator with cold finger glass condenser for use with ice or dry ice for volatile or low boiling solvents. No cooling water required. Unique drain to empty the large 1 litre trap very easily. For each condenser pattern, there is also a ...
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